
Reaction vessel | 350 mL, Teflon® |
Operating temperature | 60-250 °C (140-482 °F) |
Pressure range | 1-20 bar (2 MPa, 290 psi) |
Temperature increase | 0.5-4 °C/sec, solvent dependent |
Power range | 0-1200 W |
Agitation | Overhead Stirrer |
Cooling | Gas cooling, instant adiabatic flash cooling |
System control and data management | Windows XP® operating system, PIV 2 GHz processor, 20 GB hard di |
Temperature | 18-32 °C (64.4-89.6 °F) |
Humidity | 20-95% RH |
Power | 220-240 VAC, 50 Hz, 1ø (EU) 208 VAC, 50/60 Hz, 2ø (US, JPN) |
Air supply | > 60 lit/min, 5-10 bar |
Water supply (used to cool magnetron) | 1-3 lit/min |
Weight | < 450 kg (985 lbs) |
Dimensions | 55” x 26” x 73” W x D x H (140 cm x 65 cm x 185 cm) |
Three extra vessel entry ports | Two standard Upchurch Scientific® HPLC connections and one Swage |
Advancer Kilobatch provides up to 12 hours unattended processing of homogenous reaction mixtures delivering kilogram quantities of your target compound. In addition, the system
will accommodate heterogeneous reactions by processing four sequential cycles (250 mL) to yield a 1 L batch. Through simple solid loading replenishment, kilogram quantities of
complex heterogeneous reactions are easily achieved.
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Product Notes
Biotage® Initiator+ is top contender in a review paper on the current market offerings in microwave assisted organic synthesis (MAOS) and its applications. The huge number of microwave...
19 March 2008(March 18, 2008) Biotage, a leading supplier of tools and technology for medicinal and analytical chemistry, announces the introduction of the new Advancer® Kilobatch large-scale automated sequ...
Biotage® Advancer Kilobatch provides up to 12 hours unattended processing of homogeneous reaction mixtures delivering kilogram quantities of your target compound. In addition, the system will accommodate heterogeneous reactions by processing four sequential cycles (250 mL) to yield a 1 L batch. Through simple solid loading replenishment, kilogram quantities of complex heterogeneous reactions are easily achieved.
Specifically designed so that methods developed in Biotage lab-scale systems can be safely and predictably transferred to a larger scale without re-optimization. Powerful mechanical stirring (up to 1000 rpm) In addition to homogeneous reactions, the system also supports heterogeneous reactions and the use of solid catalysts, heavy slurries and crystallizing products.
The patent pending, "instant", adiabatic cooling promotes high purity and yield. For example, 200 mL of EtOH can be cooled from 180 °C to 65 °C in just 30 seconds.
Powerful (0-1200 W) focused magnetron rapidly heats large volumes. Dynamic Field Tuning™ minimizes reflected microwave energy.
Allows in-situ sampling during run, addition of reagents (better control of exothermals), or the creation of inert atmospheric conditions. Adaptable for real-time reaction monitoring through e.g. Raman spectroscopy.
Breech lock closure with pressure release valve and automated safety interlock, ensure maximum operator safety. System pressure control rated up to 20 bar.