Part No: AN080-HORIssued year: 2015File size: 1.18mbFile type: pdf
This application note demonstrates the use of automated solid phase extraction for a variety of pharmaceutical compounds in drinking water,
wastewater and surface water. The criteria specified in US EPA Method 1694 was met, even at very low concentrations. For lower concentrations a larger sample of water may be processed.
Part No: AN115-HORIssued year: 2017File size: 2.3mbFile type: pdf
Pesticides have gone far in increasing food supply, important in a world expecting to have 9.8 billion people by 2050. However, the mechanisms that make pesticides effective in eliminating pests can also cause harm to humans and animals. News stories continue to point to contamination through spills and exposure through the respiratory system.
Part No: AN120-HORIssued year: 2017File size: 1.44mbFile type: pdf
Polycyclic aromatic hydrocarbons (PAHs) can be found in a number of water types, such as drinking water, surface water, ground water and wastewater. There are serval types of extraction techniques that can be implemented to remove them from water for measurement including liquid-liquid extraction (LLE), continuous liquid-liquid extraction (CLLE) and solid phase extraction (SPE). With LLE and CLLE there is little selectivity within the methods for difficult matrices or other compound interferences.
Part No: PPS577Issued year: 2019File size: 1.03mbFile type: pdf
The Biotage® VacMaster™ Disk is a unit for performing manual, disk-based extractions designed for high productivity laboratories. This unit is an excellent first step for labs interested in moving from liquid-liquid extraction (LLE) to solid phase extraction (SPE) for sample preparation in the environmental, food and beverage, and agriculture industries.
Part No: AN022-HORIssued year: 2009File size: 0.91mbFile type: pdf
EPA Method 1657 describes the procedure to determine low ppb levels of organophosphorous pesticides in wastewater.
The disks compared in this study are: “Certified for Automation” Atlantic™ C18 (47 mm) and 3M Empore™ High Performance Extraction Disk C18 (47 mm).
Part No: AN018-HORIssued year: 2010File size: 0.9mbFile type: pdf
EPA Method 608 describes the procedure to determine low parts per billion levels of organochlorine pesticides, polychlorinated biphenyls, toxaphene and chlordane in wastewater. The laboratory that collected the data presented in this application note uses EPA method 608 ATP3M0222 as the approved SPE technique for waste water extraction.
The disks compared in this study are : “Certified for Automation” Atlantic™ C18 (47 mm) and 3M Empore™ High Performance Extraction Disk C18 (47 mm). Comparisons were made using side-by-side extraction and identical calibration parameters.
Part No: AN024-HORIssued year: 2012File size: 0.86mbFile type: pdf
The purpose of this application is to demonstrate the viability of a solid phase extraction (SPE) method utilizing the Horizon Technology SPE-DEX 1000/3000XL Controller with application firmware version 2.2 to extract samples for EPA Method 1664A/B and fulfill all QC requirements.
Part No: AN019-HORIssued year: 2010File size: 0.92mbFile type: pdf
The City of Fort Worth, Water Department conducted an evaluation of the Atlantic™ solid phase extraction (SPE) C18 disks using EPA Method 608. This application note describes the procedure to determine low ppb levels of organochlorine pesticides and PCBs in wastewater. This procedure used methylene chloride as the primary extraction solvent, followed by a hexane solvent exchange. Extracts were then analyzed by GC/ECD using a pressure pulse injection technique.
Part No: AN021-HORIssued year: 2020File size: 2.65mbFile type: pdf
Method 1657 describes the procedure to determine low ppb levels of organophosphorus pesticides in municipal and industrial wastewater.
The City of Fort Worth Water Department implemented Automated SPE for the analysis of organophosphorous pesticides by EPA Method 1657, using the Atlantic™ C18 solid phase extraction disk.
The Biotage® Horizon 4790 Automated Extraction System with Envision®
Platform controller, and the DryVap® Automated Drying
and Concentration System were used in this application note.
Part No: AN948Issued year: 2020File size: 0.17mbFile type: pdf
The purpose of this application note is to provide an in-line extraction and drying solution for measuring hexane extractable material (HEM) using solid-phase extraction. The extracts are dried in-line during extraction using ISOLUTE® Sodium Sulfate Drying Cartridges. Using the Speed-Vap®, the extracts are then concentrated with gentle heat and consistent air flow, and HEM concentration is determined gravimetrically.
Part No: AN930Issued year: 2020File size: 0.68mbFile type: pdf
This application note demonstrates recoveries of all the analytes within tables 1–2 of EPA method 625.1 (plus a few analytes from table 3) obtained using the Biotage® Horizon 5000 with Atlantic® 8270 One Pass solid phase extraction disks, 8270 Carbon Cartridges Max-Detect cartridges, and 1.0 Micron Atlantic® Fast Flow Pre-Filters for analyte extraction. The DryDisk® Solvent Drying System and the TurboVap® II are used for solvent drying and concentration and analysis is by GC-MS.
Part No: AN920.V.1Issued year: 2019File size: 1.14mbFile type: pdf
This application note describes the use of the Biotage® VacMaster™ Disk to extract n-hexane-extractable materials (HEM) from wastewaters per EPA Method 1664B. The procedure outlined in this document was used to generate a minimum level of quantitation (ML) and an initial demonstration of capability (IDC). Data for those studies is presented here.
Part No: AN123-HOR.V.1Issued year: 2017File size: 2.46mbFile type: pdf
The US EPA monitors a variety of chemicals in water that may cause harm to humans or wildlife in order to minimize exposure. Method 625 was developed by the Office of Science and Technology in the Clean Water program to monitor a large suite of semivolatile chemicals in wastewater for compliance with the National Pollution Discharge Elimination System (NPDES). NPDES is a system of permitting that regulates the characteristics of water that is released into a waterway, defined by industrial category. The permitting levels are set depending on the waterway’s use.
Part No: AN942Issued year: 2020File size: 1.63mbFile type: pdf
The purpose of this application note is to optimize the solution for the removal and testing of total n-hexane extractable material (HEM) using solid phase extraction in combination with the Biotage® Horizon 5000 automated extraction system.
Part No: AN102-HOR.V.2Issued year: 2016File size: 1.49mbFile type: pdf
n-Hexane-extractable material (HEM), often termed oil & grease, is an operationally-defined general measurement used around the world to help assess water pollution due to a variety of hydrocarbons, including dissolved aromatics, benzene, toluene, xylene and dispersed polynuclear aromatic hydrocarbons (PAHs), aliphatics, naphthenic and fatty acids.1
Part No: AN091-HOR.V.1Issued year: 2014File size: 4.14mbFile type: pdf
US EPA method 6251 is used to determine acidic, basic, and neutral semi-volatile organic compounds (SVOC) in municipal and industrial wastewater using GC/MS, in many cases for National Pollution Discharge Elimination System (NPDES) compliance. In method 625 revision A, the method is applied to a total possible list of 364 compounds that include; polynuclear aromatic hydrocarbons, chlorinated hydrocarbons, pesticides, phthalate esters, organophosphate esters, nitrosamines, haloethers, aldehydes, ethers, ketones, anilines, pyridines, quinolones, aromatic nitro compounds, and phenols.
Part No: AN121-HORIssued year: 2017File size: 1.67mbFile type: pdf
Environmental methods for water analysis often specify sampling 1 L of water to provide the sensitivity needed for determination of contaminants at low concentrations for health monitoring. In the past decade sensitivity of the analytical technique (GC/MS) has improved and with split/splitless introduction and large volume injection options a wide range of concentrations can be effectively measured.
Part No: AN117-HORIssued year: 2017File size: 4.2mbFile type: pdf
The US EPA monitors a variety of chemicals in water that may cause harm to humans or wildlife to minimize exposure. Method 625 was developed by the Office of Science and Technology in the Clean Water program to monitor a large suite of semivolatile chemicals in wastewater for compliance with the National Pollution Discharge Elimination System (NPDES).