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How do I purify my high boiling solvent reaction mixture using silica flash chromatography?
Small Molecules and Synthetic Therapeutics
How do I purify my high boiling solvent reaction mixture using silica flash chromatography?
Why can’t I reproduce my TLC separation using flash column chromatography?
Small Molecules and Synthetic Therapeutics
This post discusses options to separate and purify compounds by flash chromatography when TLC conditions have not successfully worked.
How does mobile phase organic solvent choice impact reversed-phase flash column chromatography?
Small Molecules and Synthetic Therapeutics
This post discusses the role that the organic solvent plays in reversed-phase separation performance.
Why is Solvent Evaluation by TLC Important for Good Flash Chromatography Results?
Small Molecules and Synthetic Therapeutics
This post shows the benefits achievable when various solvents from different selectivity groups are used for method development using TLC.
When Should I Replace My Flash C18 Column?
Small Molecules and Synthetic Therapeutics
This post discusses the criterial for determining when to replace a used C18 column.
What is Orthogonal Flash Chromatography and Why Should I do it?
Small Molecules and Synthetic Therapeutics
This post shows the benefits obtained by purifying a reaction mixture using both normal- and reversed-phase flash chromatography.
Do It Yourself: Flash Chromatography Test Mix
Small Molecules and Synthetic Therapeutics
Learn more from our in-house service expert about how to create your own Flash Chromatography Test Mix for your flash system!
How to avoid sample blowback when liquid loading
Small Molecules and Synthetic Therapeutics
This post describes some troubleshooting and remedies for sample blowback after a liquid injection with a syringe.
How to isolate impurities from a reaction product
Small Molecules and Synthetic Therapeutics
This post describes options available to remove contamination from both synthetic and natural products.
Why Reusing Flash Cartridges is Bad Science
Small Molecules and Synthetic Therapeutics
This post discusses the challenges chemists can face when reusing silica columns.
