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Microwave synthesis in the teaching laboratory
Small Molecules and Synthetic Therapeutics
Microwave reaction tutorial.
Can reaction solvent choice impact synthesis results?
Small Molecules and Synthetic Therapeutics
This post describes how the choice of a reaction solvent can influence its outcome.
How can flash chromatography UV absorbance spectra be used to identify purified compounds?
Small Molecules and Synthetic Therapeutics
This post discusses the benefits provided by PDA-UV detector for determining peak purity.
Non-aqueous (or nearly so) reversed-phase flash column chromatography – a nice alternative for purifying lipophilic compounds
Small Molecules and Synthetic Therapeutics
This post discusses the reversed-phase purification of highly lipohilic compounds using high organic content mobile phases.
How does media pore size impact peptide resolution?
Small Molecules and Synthetic Therapeutics
The stationary phase properties directly impacts your purification. Read more to learn about using large-pored particles for improved ...
How does media pore size impact small-molecule flash column chromatography?
Small Molecules and Synthetic Therapeutics
This post discussed the impact of media pore size on small-molecule flash column chromatography.
Can reversed-phase chromatography compound elution volume/time be predicted?
Small Molecules and Synthetic Therapeutics
This posts describes tips to improve reversed-phase method development.
When should I add acid to my detector make-up solvent when using mass-directed flash chromatography?
Small Molecules and Synthetic Therapeutics
When should I add acid to my detector make-up solvent when using mass-directed flash chromatography?
Invest 10 minutes on TLC and save a day of grief
Small Molecules and Synthetic Therapeutics
This post discusses the benefits of spending only 10 minutes developing TLC data to support optimized flash chromatography.
Does high performance flash column chromatography require high performance TLC for method development?
Small Molecules and Synthetic Therapeutics
Does high performance flash column chromatography require high performance TLC for method development?
